Emulsion Polymerization Reactor Online Lab Store

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Emulsion Polymerization Reactor

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  • The Emulsion Polymerisation Set Up is used to carry out the emulsion polymerization involving polymerization of an unsaturated monomer like styrene.
  • Emulsion is of the type oil in water, monomer is oil soluble & the initiator is water-soluble & an emulsifier is used to create a stable emulsion.
  • Apparatus can be used to generate the kinetic data for emulsion polymerization under various operating conditions like temperature, emulsifier concentration etc.
  • Polymerization is carried out under the atmosphere of air free nitrogen.
  • The set-up consists of jacketed type ss reactor fitted with a variable speed agitator & baffles.
  • Hot water from a digitally controlled water bath is circulated in the jacket using a pump.
  • Metered quantity of nitrogen gas from a cylinder passes through a de-oxygenation column & allowed to enter in the reactor.
  • Air has to be evacuated using a vacuum pump to create vacuum up to 30mm of hg before passing the nitrogen supply.
  • Initiator from reservoir is supplied to the reactor under pressure.
  • Set-up is complete & self-contained with sampling ports.

 

  • Experimentation:-
  • The Parameter Studies are Conducted Involving Studies of
  • Effect of Rpm on Conversion
  • Effect of Initiator Concentration
  • Effect of Monomer Concentration
  • Effect of Emulsifier Concentration
  • Utilities Required
  • Water Supply and Drain
  • Electricity-1.5 kW, Single
  • Instruments, Laboratory Wares and Chemicals Required for Analysis as per the System Adopted
  • Vacuum Pump
  • High Purity N2 Gas
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